Conclusions
The acid chlorides of thiophosphorous and thiophosphonous acids react with trimethylsilyi cyanide to give the corresponding trivalent phosphorus thiocyanides, which give theα-cyanoalkyl esters of phosphorus thioacids when reacted with carbonyl compounds.
Literature cited
A. N. Pudovik, G. V. Romanov, E. N. Ofitserov, V. P. Kukhar', V. N. Volkova, L. A. Lazukina, and G. I. Khaskin, USSR Patent 771,107 (1978); Byull. Izobr., No. 38 (1980).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 939–940, April, 1982.
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Pudovik, A.N., Romanov, G.V. & Volkova, V.N. Trivalent phosphorus thiocyanides. Russ Chem Bull 31, 831–832 (1982). https://doi.org/10.1007/BF00950033
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DOI: https://doi.org/10.1007/BF00950033