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Preparation of N-phosphorylated and silylated 1,3,2-oxaza(diaza)phospholanes and phosphorinanes

  • M. A. Pudovik
  • N. P. Morozova
  • M. D. Medvedeva
  • A. N. Pudovik
Brief Communications
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Conclusions

  1. 1.

    The reaction of N-phenyl(benzyl)ethylenediamine with the full amides of phosphorous acid gave a number of N-phosphorylated 1,3,2-diazaphospholanes.

     
  2. 2.

    The reaction of alkanolamines with the diamides of alkylphosphorous acids, followed by treatment with trimethylsilyldiethylamine in the presence of catalytic amounts of ammonium sulfate, gave N-silylated 1,3,2-oxazaphospholanes and phosphorinanes.

     

Keywords

Sulfate Ammonium Amide Phosphorous Acid Benzyl 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Literature cited

  1. 1.
    G. Bentrude, W. D. Johnson, and W. A. Khan, J. Am. Chem. Soc.,94, 923 (1972).Google Scholar
  2. 2.
    M. A. Pudovik, S. A. Terent'eva, Yu. Yu. Samitov, and A. N. Pudovik, Zh. Obshch. Khim.,46, 266 (1975).Google Scholar
  3. 3.
    M. A. Pudovik, S. A. Terent'eva, and A. N. Pudovik, Zh. Obshch. Khim.,45, 518 (1975).Google Scholar

Copyright information

© Plenum Publishing Corporation 1979

Authors and Affiliations

  • M. A. Pudovik
    • 1
  • N. P. Morozova
    • 1
  • M. D. Medvedeva
    • 1
  • A. N. Pudovik
    • 1
  1. 1.A. E. Arbuzov Institute of Organic and Physical ChemistryKazan Branch of the Academy of Sciences of the USSRUSSR

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