Conclusions
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1.
The selective removal of protective groups was studied for some 0-(aminoalkyl)hydroxylamines, and a method for the functional analysis of the obtained compounds was discussed.
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2.
Starting with a BrCN-activated Sepharose we obtained some sorbents that carry 0-substituted hydroxylamine moieties.
Literature cited
A. A. Nedospasov and R. M. Khomutov, Izv. Akad. Nauk SSSR, Ser. Khim.,1976, 1136.
A. A. Nedospasov and R. M. Khomutov, Izv. Akad. Nauk SSSR, Ser. Khim.,1978, 962.
R. Axen, J. Porath, and S. Ernback, Nature,214, 1302 (1967).
L. Kagedal and S. Akerström, Acta Chem. Scand.,24, 1601 (1970).
P. Cuatrecasas, J. Biol. Chem.,245, 3059 (1970).
A. A. Nedospasov and R. M. Khomutov, Third All-Union Conference on Analytical Chemistry of Organic Compounds, Abstracts of Papers [in Russian], Nauka (1976), p. 43.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 10, pp. 2397–2400, October, 1978.
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Nedospasov, A.A., Khomutov, R.M. Use of N-protected aminoalkoxyamines in synthesis of aminooxy adsorbents using BrCN. Russ Chem Bull 27, 2130–2132 (1978). https://doi.org/10.1007/BF00946544
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DOI: https://doi.org/10.1007/BF00946544