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Use of acetal protection to synthesize cyclopropane alcohols

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

The reaction of dichlorocarbene with the bis(1,3-pentadienyl) acetal of acetaldehyde under the conditions of a two-phase system is nonselective when a twofold excess of chloroform is used.

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Literature cited

  1. M. Makosza and M. Wawrzyniewicz, Tetrahedron Lett., 4659 (1969).

  2. A. Kh. Khusid, G. V. Kryshtal' (Kryshtal), V. F. Kucherov, and L. A. Yanovskaya (Janovskaya), Synthesis, 428 (1977).

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  4. A. Kh. Khusid, G. V. Kryshtal', V. F. Kucherov, and L. A. Yanovskaya, Izv. Akad. Nauk SSSR, Ser. Khim., 2135 (1977).

  5. A. Kh. Khusid, G. V. Kryshtal', V. F. Kucherov, and L. A. Yanovskaya, Izv. Akad. Nauk SSSR, Ser. Khim., 692 (1977).

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow

    G. V. Kryshtal', V. F. Kucherov & L. A. Yanovskaya

Authors
  1. G. V. Kryshtal'
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  2. V. F. Kucherov
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  3. L. A. Yanovskaya
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2806–2808, December, 1978.

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Kryshtal', G.V., Kucherov, V.F. & Yanovskaya, L.A. Use of acetal protection to synthesize cyclopropane alcohols. Russ Chem Bull 27, 2506–2508 (1978). https://doi.org/10.1007/BF00941111

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  • DOI: https://doi.org/10.1007/BF00941111

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