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α-Phenyl-β-diethyl(diphenyl)phosphonohydrazines

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    Instead of the expected α-phenyl-β-diethyl(diphenyl)phosphonohydrazine, the α-phenyl-β-diethyl (diphenyl)phosphonohydrazines were obtained when the acid chlorides of the diethyl(diphenyl) phosphates are reacted with the unsymmetrical sodium phenylhydrazine in absolute benzene medium.

  2. 2.

    The reaction of the dichloride of phthalic acid with the a-phenyl-β-diethyl(diphenyl)phosphonohydrazines in absolute benzene medium, in the presence of triethylamine, respectively gave 2-phenyl-3-diethylphosphono-1,4-phthalazinedione and 2-phenyl-3-diphenylphosphono-1,4-phthalazinedione.

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Literature cited

  1. A. E. Arbuzov, F. G. Valitova, A. V. Il'yasov, B. M. Kozyrev, and Yu. V. Yablokov, Dokl. Akad. Nauk SSSR,147, 839 (1962).

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Deceased.

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1646–1648, July, 1973.

The authors express their sincere gratitude to R. R. Shagidullin for studying the IR spectra.

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Arbuzov, A.E., Valitova, F.G., Gazetdinova, N.G. et al. α-Phenyl-β-diethyl(diphenyl)phosphonohydrazines. Russ Chem Bull 22, 1594–1596 (1973). https://doi.org/10.1007/BF00930071

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  • DOI: https://doi.org/10.1007/BF00930071

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