Synthesis of α-sulfur-containing 2-imidazolinone derivatives

  • S. I. Zav'yalov
  • O. M. Radul
  • V. I. Gunar
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Conclusions

  1. 1.

    A method was developed for the synthesis ofα-sulfur-containing derivatives of 2-imidazolinone by the reaction of 4(5)-piperidino-methyl-2-imidazolinones with mercaptans, carbon disulfide and thioacetic acid.

     
  2. 2.

    4(5)-Methyl-5(4)-S-acetylmercaptomethyl-2-imidazolinone was converted to bis[4(5)-methyl-2-imidazolinonyl-5(4)-methyl] sulfide under the influence of piperidine.

     

Keywords

Methyl Sulfide Disulfide Piperidine Carbon Disulfide 

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Literature cited

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    N. A. Rodionova, M. P. Unanyan, G. V. Kondrat'eva, S. I. Zav'yalov, and V. V. Filippov, Izv. Akad. Nauk SSSR, Ser. Khim.,1970, 660.Google Scholar
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    S. I. Zav'yalov, O. M. Radul, and N. A. Rodionova, Izv. Akad. Nauk SSSR, Ser, Khim.,1972, 2025.Google Scholar
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    S. I. Zav'yalov, M. P. Unanyan, G. V. Kondrat'eva, and V. I. Filippov, Izv. Akad. Nauk SSSR, Ser. Khim.,1967, 1792.Google Scholar

Copyright information

© Consultants Bureau 1973

Authors and Affiliations

  • S. I. Zav'yalov
    • 1
  • O. M. Radul
    • 1
  • V. I. Gunar
    • 1
  1. 1.N. D. Zelinskii Institute of Organic ChemistryAcademy of Sciences of the USSRUSSR

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