Advertisement

Separation of organic compounds and their deuterated analogs by preparative gas chromatography

  • M. P. Zabokritskii
  • B. A. Rudenko
  • V. P. Chizhkov
Brief Communications
  • 49 Downloads

Conclusions

Using the circulation GLC method we were able to effect the preparative separation of some ordinary and fully deuterated products with an efficiency that is comparable to that achieved using capillary chromatography and exceeds 40 thousand theoretical plates.

Keywords

Chromatography Organic Compound Theoretical Plate Preparative Separation Capillary Chromatography 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literature cited

  1. 1.
    Preparative Gas Chromatography [in Russian], Mir (1974).Google Scholar
  2. 2.
    K. I. Sakodynskii and S. A. Volkov, Preparative Gas Chromatography [in Russian], Nauka (1971).Google Scholar
  3. 3.
    M. Verzele, J. Gas. Chromatogr.,4, 180 (1966).Google Scholar
  4. 4.
    B. A. Rudenko, V. A. Kuzovkin, V. N. Paukov, and V. F. Kucherov, Izv. Akad. Nauk SSSR, Ser. Khim., 1384 (1971).Google Scholar
  5. 5.
    V. P. Chizhkov, I. Samogil, and E. P. Skornyakov, USSR Patent 160363, Dec. 6, 1961; Byull. Izobr., No. 3, 67 (1964).Google Scholar
  6. 6.
    V. P. Chizhkov, E. F. Litvin, M. I. Usorov, L. M. Yakushina, and A. A. Matyukov, Izv. Akad. Nauk SSSR, Ser. Khim., 1154 (1971).Google Scholar
  7. 7.
    V. P. Chizhkov, M. I. Usorov, and L. A. Sinitsina, Zavod. Lab.,37, 1286 (1971).Google Scholar
  8. 8.
    V. P. Chizhkov, B. A. Rudenko, L. A. Sinitsina, and G. A. Yushina, Izv. Akad. Nauk SSSR, Ser. Khim., 1207 (1975).Google Scholar
  9. 9.
    V. P. Chizhkov, G. A. Yushina, L. A. Sinitzina (Sinitsina), and B. A. Rudenko, J. Chromatogr.,120, 35, (1976).Google Scholar
  10. 10.
    R. Yaris and J. R. Sams, J. Chem. Phys.,37, 571 (1962).Google Scholar

Copyright information

© Plenum Publishing CorporationPlenum Publishing Corporation 1978

Authors and Affiliations

  • M. P. Zabokritskii
    • 1
  • B. A. Rudenko
    • 1
  • V. P. Chizhkov
    • 1
  1. 1.N. D. Zelinskii Institute of Organic ChemistryAcademy of Sciences of the USSRMoscow

Personalised recommendations