Conclusions
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1.
A number of new sulfur-containing organosilicon monomers was synthesized by the reaction of 1,2-bis(alkylmethoxysilyl)- and 1-(trimethylsilyl)-2-(methylmethoxysilyi)ethylenes with mercaptans and thioacetic acid.
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2.
Based on the NMR spectral data, the 1-(trimethylsilyl)-2-(methylmethoxysilyl)ethylenes form two isomeric adducts in a 1∶1 ratio.
Literature cited
N. V. Komarov, O. G. Yarosh, L. P. Vakhrushev, and N. F. Chernov, Zh. Obshch. Khim.,40, 1171 (1970).
N. V. Komarov, Z. I. Mikhailov, O. G. Yarosh, L. P. Vakhrushev, N. F. Chernov, and L. F. Ul'yanova, Izv. Akad. Nauk SSSR, Ser. Khim., 2581 (1971).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No.1, pp.171–175, January, 1976.
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Voronkov, M.G., Tsvetaeva, L.V., Sigalov, M.V. et al. Photochemical thiylation of Si-methoxy-substituted 1, 2-disilylethylenes. Russ Chem Bull 25, 160–163 (1976). https://doi.org/10.1007/BF00925642
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DOI: https://doi.org/10.1007/BF00925642