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Preparation of O-(polyfluoroalkyl) alkylchlorophosphonates and O-(polyfluoroalkyl) aryl chlorophosphates by catalytic phosphorylation of polyfluoroalkanols

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

A new method was developed for the synthesis of O-(polyfluoroalkyl) alkylchlorophosphonates and 0-(polyfluoroalkyl) aryl chlorophosphates, which consists in phosphorylating polyfluoroalkanols with an excess of the dichlorides of the corresponding phosphorus acids in the presence of salts of the Group II metals.

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Literature cited

  1. M. I. Kabachnik, N. N. Godovikov, V. V. Pisarenko, and L. S. Zakharov, Izv. Akad. Nauk SSSR, Ser. Khim.,1972, 1667.

  2. L. S. Zakharov, V. V. Pisarenko, N. N. Godovikov, and M. I. Kabachnik, Izv. Akad. Nauk SSSR, Ser. Khim.,1971, 2503.

  3. Kh. R. Raver and G. I. Abramtseva, USSR Inventor's Certificate No. 203,680, Aug. 31, 1966; Byull. Izobr., No. 21, 29 (1967).

  4. M. I. Kabachnik, L. S. Zakharov, E. I. Goryunov, I. Yu. Kudryavtsev, A. P. Kharchenko, V. F. Zabolotskikh, G. D. Novikova, K. N. Bil'dinov, and A. I. Nikitina, USSR Inventor's Certificate No. 556,148, July 12, 1976; Byull. Izobr., No. 16, 68 (1977).

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Authors and Affiliations

  1. Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow

    M. I. Kabachnik, L. S. Zakharov, E. I. Goryunov, A. P. Kharchenko, V. F. Zabolotskikh, G. D. Novikova & V. A. Svoren

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  1. M. I. Kabachnik
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  2. L. S. Zakharov
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  3. E. I. Goryunov
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  4. A. P. Kharchenko
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  5. V. F. Zabolotskikh
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  6. G. D. Novikova
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  7. V. A. Svoren
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 656–658, March, 1979.

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Kabachnik, M.I., Zakharov, L.S., Goryunov, E.I. et al. Preparation of O-(polyfluoroalkyl) alkylchlorophosphonates and O-(polyfluoroalkyl) aryl chlorophosphates by catalytic phosphorylation of polyfluoroalkanols. Russ Chem Bull 28, 611–613 (1979). https://doi.org/10.1007/BF00924850

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  • DOI: https://doi.org/10.1007/BF00924850

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