Conclusions
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1.
The reaction of ɛ-caprolactam with epichlorohydrin leads to the formation of ɛ-caprolactam-1-chloro-2-propanol, which is converted to 2,3-epoxypropyl-N-ɛ-caprolactam by treatment with NaOH.
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2.
The reaction of ɛ-caprolactam with γ-glycidoxytrimethylenetriethoxysilane gave a polymeric product, which begins to lose weight only at 280°, while the weight loss at 350° does not exceed 10–12%.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 665–667, March, 1978.
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Andrianov, K.A., Nogaideli, A.I., Khananashvili, L.M. et al. Reaction of ɛ-caprolactam with epichlorohydrin and γ-glycidoxytrimethylenetriethoxysilane. Russ Chem Bull 27, 573–574 (1978). https://doi.org/10.1007/BF00923941
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DOI: https://doi.org/10.1007/BF00923941