Conclusions
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1.
A method was developed for the synthesis of methoxymethylhexachloroantimonate, in which connection all of the operations were carried out in vacuo.
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2.
The decomposition into molecular forms, which is characteristic for MMH solutions, depends to a large degree on the polarity of the medium.
Literature cited
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Yu. V. Pokonova, Halo Ethers [in Russian], Khimiya (1966).
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G. A. Olah, J. J. Svoboda, and J. A. Olah, Synthesis, 544 (1972).
Yu. N. Smirnov, B. A. Komarov, V. P. Volkov, and É. F. Oleinik, Abstracts of the Eighteenth Conference on High-Molecular Compounds [in Russian], Kazan' (1973), p. 51; B. A. Komarov, V. P. Volkov, and B. A. Rozenberg, ibid., p. 51.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 8, pp. 1874–1876, August, 1974.
The NMR spectra were taken by I. S. Morozova and G. N. Boiko, for which the authors express their gratitude.
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Komarov, B.A., Rozenberg, B.A. & Enikolopyan, N.S. Synthesis of methoxymethylhexachloroantimonate. Russ Chem Bull 23, 1795–1797 (1974). https://doi.org/10.1007/BF00923215
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DOI: https://doi.org/10.1007/BF00923215