Conclusions
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1.
The reaction of diethylamidophosphorous dichloride with propylene sulfide at 100–110° leads to formation of diethylamidothiophosphoryl dichloride, diethylamido-β-chloropropylthiophosphorous chloride, and diethylamido-β-chloropropyldithiophosphoryl chloride.
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2.
In the case of ethylene sulfide, diethylamido-β-chloroethylthiophosphorous chloride mainly is formed.
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Literature cited
O. N. Nuretdinova, Izv. Akad. Nauk SSSR, Ser. Khim., 1901 (1965).
O. N. Nuretdinova, ibid., 1255 (1966).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 5, pp. 1125–1128, May, 1969.
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Nuretdinova, O.N., Nikonova, L.Z. Reaction of diethylamidophosphorous bichloride with alkylene sulfides. Russ Chem Bull 18, 1028–1030 (1969). https://doi.org/10.1007/BF00922864
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DOI: https://doi.org/10.1007/BF00922864