Conclusions
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1.
A series of nitroxyl radicals -products of the addition of shortlived radicals [(NO2)3Ċ, CH3Ċ(NO2)2, (CH3)2ĊNO2, (CH3)3C., (CH3)3CO, ho. and N3 .] to phenyl-tert-butylnitrone, used as radical trap — was produced. The identification of the nitroxyl radicals obtained was performed on the basis of an analysis of the ESR spectra, using the method of countersynthesis.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 11, pp. 2436–2443, November, 1975.
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Okhlobystina, L.V., Tyurikov, V.A., Shapiro, B.I. et al. Investigation of the formation of free radicals in reactions of aliphatic nitro compounds by the method of radical traps. Russ Chem Bull 24, 2323–2329 (1975). https://doi.org/10.1007/BF00921641
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DOI: https://doi.org/10.1007/BF00921641