Conclusions
The combined use of the1H and13C NMR spectra makes it possible to unequivocally assign the 1,4,5-trimethyl-4-cyclohexene-1,2-dicarboxylic acids and their derivatives to a given steric series.
Literature cited
D. M. Bailey and R. E. Johnson, J. Org. Chem.,35, 3574 (1970).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 8, pp. 1892–1894, August, 1976.
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Denisenko, V.A., Novikov, V.L., Isakov, V.V. et al. Use of1H and13C NMR spectroscopy to determine the stereochemistry of 1,4,5-trime thyl-4-cyclohexene-1,2-dicarboxylic acids and their derivatives. Russ Chem Bull 25, 1782–1784 (1976). https://doi.org/10.1007/BF00921460
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DOI: https://doi.org/10.1007/BF00921460