Conclusions
-
1.
The synthesis has been accomplished of the methylamides ofα-N-benzoyl-β-(N′-methyl-N″-phenyl-thiocarbamyl)propionic ] and butyric acids, which under the conditions used for dehydration of polypeptide chains by the Edman method through treatment with trifluoroacetic acid were converted into cyclic derivatives of hexahydropyrimidine.
-
2.
Derivatives of D, L-erythro- and D, L-threo-diaminobutyric acid were readily and reversibly converted into one another under the action of acidic and basic reagents.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
Literature cited
Z. I. Lebedeva, L. A. Baratova, S. M. Avaeva, I. V. Medvedeva, M. N. Mirzayanova, and A. Ya. Khorlin, Bioorgan. Khim.,1, 923 (1975).
L. A. Baratova, V. A. Sklyankina, V. Yu. Kolesnikova, and S. M. Avaeva, J. Chromatogr.,70, 162 (1972).
E. Fischer and K. Raske, Ber.,40, 3723 (1907).
M. Kinoshita and S. Umezava, J. Chem. Soc. Japan, Pure Chem. Sec.,72, 382 (1951).
E. P. Painter, J. Amer. Chem. Soc.,69, 229 (1947).
S. M. Avaeva, V. A. Sklyankina, L. V. Ermolenko, and M. M. Botvinik, Zh. Obshch. Khim.,38, 2363 (1968).
Author information
Authors and Affiliations
Additional information
Translated from Izvestiya Akademii Nauk SSSR, Seriya Khmicheskaya, No. 7, pp. 1603–1608, July, 1976. ]
The authors express their thanks to L. B. Senyavina for recording and discussing the IR spectra and to S. A. Koz'min and T. A. Balasheva Likewise for the PMR spectra.
Rights and permissions
About this article
Cite this article
Mirzayanova, M.N., Medvedeva, I.V., Fedulova, I.E. et al. Synthesis and properties of derivatives of diaminopropionic and diaminobutyric acids. Russ Chem Bull 25, 1520–1524 (1976). https://doi.org/10.1007/BF00920830
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF00920830