Summary
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1.
Triallylborine reacts with triisobutylborine with formation of a polymeric product.
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2.
Treatment of the polymer with alcohols gives 1,5-dialkoxy-1,5-diborocanes.
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3.
Treatment of 1,5-dibutoxy-1,5-diborocane with phosphorus pentachloride gives 1,5-dichloro-1,5-diborocane.
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4.
1,5-Dichloro-1,5-diborocane reacts with ethylamine with formation of N,N*-diethyl-1,5-diborocane-1,5-diamine.
Literature cited
B. M. Mikhailov and T. A. Shchegoleva, Bull. Acad. Sci. USSR, Div. Chem. Sci. (1959), 556.
B. M. Mikhailov and N. S. Fedotov, Bull. Acad. Sci. USSR, Div. Chem. Sci. (1956), 375.
B. M. Mikhailov and T. A. Shchegoleva, Bull. Acad. Sci. USSR, Div. Chem. Sci. (1956), 508.
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Mikhailov, B.M., Tutorskaya, F.B. Derivatives of 1,5-diborocane. Russ Chem Bull 8, 1091–1093 (1959). https://doi.org/10.1007/BF00916682
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DOI: https://doi.org/10.1007/BF00916682