Summary
It was shown that it is possible to prepare levoglucosan (β-D-1,6-anhydroglucopyranose) in a yield of not less than 40% by the thermodegradation of cellulose at low pressure with superheated steam as heat-transfer medium.
Literature cited
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H. I. P. Venn, J. Textile Inst. 15, 414 (1924).
I. Mutti and A. Montalti, Ann. Chim. Applicata 17, 188 (1927).
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Épshtein, Y.V., Golova, O.P. & Durynina, L.I. Preparation of levoglucosan (β-d-1,6-anhydroglucopyranose) by the thermodegradation of cellulose in a stream of superheated steam under reduced pressure. Russ Chem Bull 8, 1089–1090 (1959). https://doi.org/10.1007/BF00916681
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DOI: https://doi.org/10.1007/BF00916681