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A New synthesis op difluoroaminodifluoroacetic acid derivatives

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The reaction of tetrafluorohydrazine with vinylidene fluoride and trifluoroethylene in the presence of potassium fluoride gave difluoroaminodifluoroacetonitrile and the N-fluoroiminylfluoride of difluoroaminodifluoroacetic acid, respectively.

  2. 2.

    The nitrile and N-fluoroiminylfluoride of difluoroaminodifluoroacetic acid are transformed into the methyl ester of this acid under the influence of methanol and sulfuric acid.

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Literature cited

  1. M. Lustig and J. K. Ruff, J. Inorg. Chem.,4, 1441 (1965).

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  2. R. A. Bekker, B. L. Dyatkin, and I. L. Knunyants, Izv. AN SSSR, Ser. khim.,1967, 1960.

  3. A. L. Logothetis and G. N. Sausen, J. Org. Chem.,31, 3686 (1966).

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Authors and Affiliations

  1. Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, USSR

    B. L. Dyatkin, K. N. Makarov & I. L. Knunyants

Authors
  1. B. L. Dyatkin
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  2. K. N. Makarov
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  3. I. L. Knunyants
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 657–658, March, 1968.

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Dyatkin, B.L., Makarov, K.N. & Knunyants, I.L. A New synthesis op difluoroaminodifluoroacetic acid derivatives. Russ Chem Bull 17, 635–636 (1968). https://doi.org/10.1007/BF00911629

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  • DOI: https://doi.org/10.1007/BF00911629

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