Preparation of 1-chloro-3-methylboracyclopentane and some of its transformations
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The reaction of boron trichloride with bis-1,4-(3-methylboracyclopentyl)-2-methylbutane gave 1-chloro-3-methylboracyclopentane.
Symmetrization occurs when bis-1,4-(dichloroboron)-2-methylbutane is heated, with die formation of 1-chloro-3-methylboracyclopentane and boron trichloride.
A study was made of the replacement of the chlorine atom in 1-chloro-3-methylboracyclopentane by the alkoxy group, hydrogen, and alkyl.
KeywordsHydrogen Boron Chlorine Chlorine Atom Trichloride
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- 1.L. I. Zakharkin and A. I. Kovredov, Zh.Obshch. Khim.32, 1461 (1962); Izv. AN SSSR, Otdel, Khim, Nauk, 357, 362 (1962).Google Scholar