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Synthesis of silicon-containing acetylenic alcohols

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

  1. 1.

    Some derivatives of triethylethynylsilane were synthesized from its Grignard reagent, which was prepared in tetrahydrofuran in high yield.

  2. 2.

    By the addition of triethylsilane to 1,1,1-trifluoro-2-methyl-3-buten-2-ol the silicon- and fluorine-containing tertiary unsaturated alcohol 1,1,1-trifluoro-2-methyl-3-(triethylsilyl)-3-buten-2-ol was obtained.

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Literature cited

  1. E. Jones, L. Skatteböl, and M. Whiting, J. Chem. Soc. (1956), 4765.

  2. H. Normant and T. Guvigny, Bull. Soc. Chim. France 447 (1957).

  3. A. D. Petrov, L. L. Shukovskaia, S. I. Sadykh-Zade, and Iu. P. Egorov, Proc. Acad. Sci. USSR 115, 522 (1957).

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Authors and Affiliations

  1. Institute of Silicate Chemistry of the Academy of Sciences of the USSR, USSR

    L. L. Shchukovskaia & A. D. Petrov

Authors
  1. L. L. Shchukovskaia
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  2. A. D. Petrov
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Shchukovskaia, L.L., Petrov, A.D. Synthesis of silicon-containing acetylenic alcohols. Russ Chem Bull 7, 983–986 (1958). https://doi.org/10.1007/BF00911353

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  • DOI: https://doi.org/10.1007/BF00911353

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