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Anwendung der Hochdruck-Flüssig-Flüssig-Chromatographic (LLC) in der Metallocenchemie

The application of High Pressure Liquid-Liquid-Chromatography (LCC) in the chemistry of metallocenes

  • Organische Chemie und Biochemie
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Abstract

The High Pressure Liquid-Liquid-Chromatography (LLC) is an excellent technique for the qualitative and quantitative separation of isomeric and homologous metallocenes, as is shown with 55 various derivatives of benchrotrene, ferrocene and cymantrene.

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Literatur

  1. H. Falk, H. Lehner undK. Schlögl, J. Organomet. Chem.55, 191 (1973).

    Google Scholar 

  2. K. Schlögl, Pure and Appl. Chem.23, 413 (1970);K. Schlögl, in: Topics in Stereochemistry, Bd. 1. New York: Wiley-Interscience. 1967.

    Google Scholar 

  3. K. Schlögl undH. Falk, Ferrocene, in: Methodicum Chimicum, Bd. 8. Stuttgart: Thieme (im Druck).

  4. B. Kainradl, E. Langer, H. Lehner undK. Schlögl, Ann. Chem.766, 16 (1972).

    Google Scholar 

  5. E. Langer undH. Lehner, Tetrahedron28, 375 (1973).

    Google Scholar 

  6. B. Deubzer, H. P. Fritz, C. G. Kreiter undK. Öfele, J. Organomet. Chem.7, 289 (1967).

    Google Scholar 

  7. H. Lehner undK. Schlögl, Mh. Chem.101, 895 (1970).

    Google Scholar 

  8. K. Schlögl, H. Falk undG. Haller, Mh. Chem.98, 82 (1967).

    Google Scholar 

  9. B. Deubzer, Dissertation, Technische Hochschule München, München (1966).

  10. H. Egger undH. Falk, Mh. Chem.99, 1056 (1968);H. Egger undA. Nikiforov, Mh. Chem.99, 2296 (1968).

    Google Scholar 

  11. J. J. Kirkland (Hrsg.), Modern Practice of Liquid Chromatography. New York: Wiley. 1971.

    Google Scholar 

  12. J. M. Greenwood, H. Veening undB. R. Willeford, J. Organomet. Chem.38, 345 (1972).

    Google Scholar 

  13. B. Nicholls undM. C. Whiting, J. Chem. Soc.1959, 551.

  14. G. Natta, R. Ercoli undF. Calderazzo, Chim. e Ind. [Mailand]40, 287 (1958).

    Google Scholar 

  15. H. Falk, K. Schlögl undW. Steyrer, Mh. Chem.97, 1029 (1966).

    Google Scholar 

  16. H. Falk undK. Schlögl, Mh. Chem.99, 578 (1968).

    Google Scholar 

  17. R. Riemschneider, O. Becker undK. Franz, Mh. Chem.90, 571 (1959);R. Ercoli, F. Calderazzo undE. Mantica, Chim. e Ind. [Mailand]41, 404 (1959).

    Google Scholar 

  18. K. Schlögl undH. Egger, Ann. Chem.676, 76 (1964).

    Google Scholar 

  19. A. N. Nesmeyanov, E. G. Perevalova, R. V. Golovnya undO. A. Nesmeyanova, Dokl. Akad. Nauk SSSR97, 459 (1954); Chem. Abstr.49, 9633 h (1955).

    Google Scholar 

  20. H. Falk, G. Haller undK. Schlögl, Mh. Chem.98, 592 (1967).

    Google Scholar 

  21. G. D. Broadhead, J. M. Osgerby undP. L. Pauson, J. Chem. Soc.1958, 650.

  22. G. Haller undK. Schlögl, Mh. Chem.98, 603 (1967).

    Google Scholar 

  23. M. Rausch, M. Vogel undH. Rosenberg, J. Org. Chem.22, 903 (1957).

    Google Scholar 

  24. M. Cais, A. Modiano undA. Raveh, J. Amer. Chem. Soc.87, 5607 (1965).

    Google Scholar 

  25. D. E. Bublitz, W. E. McEwen undJ. Kleinberg, J. Amer. Chem. Soc.84, 1845 (1962).

    Google Scholar 

  26. P. Reich-Rohrwig undK. Schlögl, Mh. Chem.99, 1752 (1968).

    Google Scholar 

  27. R. Riemschneider undK. Petzoldt, Z. Naturforsch.15b, 627 (1960).

    Google Scholar 

  28. R. Riemschneider undH. G. Kassahn, Z. Naturforsch.14b, 348 (1959).

    Google Scholar 

  29. J. A. Hirsch, in: Topics in Stereochemistry, Bd. 1. New York: Wiley-Interscience. 1967.

    Google Scholar 

  30. G. Helmchen, R. Ott undK. Sauber, Tetrahedron Lett.1972, 3873.

  31. W. H. Laarhoven, Th. J. H. M. Cuppen undR. J. F. Nivard, Tetrahedron26, 4865 (1970).

    Google Scholar 

  32. W. F. Little undR. Eisenthal, J. Org. Chem.26, 3609 (1961).

    Google Scholar 

  33. I. K. Ushenko, K. D. Zhikhareva undF. Z. Rodova, Zh. Obshch. Khim.33, 798 (1963); Chem. Abstr.59, 10268 e (1963).

    Google Scholar 

  34. X. A. Dominguez, I. C. Lopez undR. Franco, J. Org. Chem.26, 1625 (1961).

    Google Scholar 

  35. S. Akabori, T. Sato undK. Hata, J. Org. Chem.33, 3277 (1968).

    Google Scholar 

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Authors and Affiliations

  1. Lehrkanzel für Organische Chemie der Universität Wien, Österreich

    R. Eberhardt, H. Lehner & K. Schlögl

Authors
  1. R. Eberhardt
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  2. H. Lehner
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  3. K. Schlögl
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Additional information

Herrn Prof. Dr.F. Hecht mit herzlichen Wünschen zum 70. Geburtstag gewidmet.

Mit 8 Abbildungen

Diese Arbeit zählen wir als 38. Mitt. über Stereochemie von Metallocenen und 59. Mitt. über Ferrocenderivate; 37. bzw. 58. Mitt. s. Ref.1. Auszugsweise vorgetragen bei der Tagung des Vereins österr. Chemiker in Linz am 28. September 1973.

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Eberhardt, R., Lehner, H. & Schlögl, K. Anwendung der Hochdruck-Flüssig-Flüssig-Chromatographic (LLC) in der Metallocenchemie. Monatshefte für Chemie 104, 1409–1420 (1973). https://doi.org/10.1007/BF00910058

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  • DOI: https://doi.org/10.1007/BF00910058

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