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On the reaction of methyl dichlorophosphine with acrylamide

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The following compounds are formed by the reaction of methyl dichlorophosphine with acrylamide: methyl-β-cyanoethylphosphonyl chloride (36.6%),β-chloropropionitrile (16.2%) and methyl-β-cyanoettylphosphonic acid (3.4%).

  2. 2.

    The reaction of methyl-β-cyanoethylphosphonyl chloride with water (2∶1) gave methyl-β-cyanoethylphosphonic acid anhydride.

  3. 3.

    By reacting methyl-β-cyanoethylphosphonyl chloride with alcohols and diethylamine, we have obtained a number of esters and the diethylamide of methyl-β-cyanoethylphosphonic acid.

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Literature cited

  1. V. K. Khairullin, M. A. Vasyanina, and A. N. Pudovik, Izv. AN SSSR, Ser. khim.,1967, 1603.

  2. Belsteins Handbuch der organischen Chemie, Berlin, 1920,2, p. 250.

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Authors and Affiliations

  1. A. E. Arbuzov Institute of Inorganic and Physical Chemistry, Academy of Sciences of the USSR, USSR

    V. K. Khairullin, R. M. Kondrat'eva & A. N. Pudovik

Authors
  1. V. K. Khairullin
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  2. R. M. Kondrat'eva
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  3. A. N. Pudovik
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 9, pp. 2097–2099, September, 1967.

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Khairullin, V.K., Kondrat'eva, R.M. & Pudovik, A.N. On the reaction of methyl dichlorophosphine with acrylamide. Russ Chem Bull 16, 2019–2021 (1967). https://doi.org/10.1007/BF00909610

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  • DOI: https://doi.org/10.1007/BF00909610

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