Summary
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1.
Triethylcyclotrisilazane and tetraethylcyclotetrasilazane were synthesized and characterized.
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2.
The ammonolysis of dichloromethylsilane gives tetramethylcyclotetrasilazane and an individual product, which consisted of condensed rings and had the empirical formula (CH3SiH)6N2(NH)3. Both products were isolated and characterized.
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US Patent 2885370, May 5, 1959.
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Semenova, E.A., Zhinkin, D.Y. & Andrianov, K.A. Synthesis of alkylcyclosilazanes containing silicon-attached hydrogen. Russ Chem Bull 11, 246–248 (1962). https://doi.org/10.1007/BF00908026
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DOI: https://doi.org/10.1007/BF00908026