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Synthesis of methyl α-nitrocrotonate

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

Methyl α-nitrocrotonate has been synthesized by the condensation of methyl nitroacetate with acetaldehyde, acetylation of the methyl α-nitro-β-hydroxybutyrate, and subsequent deacetylation of the resulting product.

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Literature cited

  1. H. Feurer, H. B. Hass, and R. S. Warren, J. Amer. Chem. Soc.71, 3078 (1949).

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  2. V. M. Rodionov and V. M. Belikov, Dokl. AN SSSR,93, 827 (1953).

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences, USSR

    I. S. Ivanova, Yu. V. Konnova & S. S. Novikov

Authors
  1. I. S. Ivanova
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  2. Yu. V. Konnova
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  3. S. S. Novikov
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Ivanova, I.S., Konnova, Y.V. & Novikov, S.S. Synthesis of methyl α-nitrocrotonate. Russ Chem Bull 11, 1591–1592 (1962). https://doi.org/10.1007/BF00907246

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  • DOI: https://doi.org/10.1007/BF00907246

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