Summary
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1.
The reaction between butylorthotitanates and dimethylcyclosiloxanes yields low-molecular weight organosilicon monomers.
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2.
A method of synthesizing the difficultly obtainable 1,3-dibutoxytetramethyldisiloxane is proposed.
Literature cited
K. A. Andrianov and Sh. V. Pichkhadze, “High-molecular Weight Compds.” [in Russian]3, 577 (1961).
K. A. Andrianov, Sh. V. Pichkhadze, and I. V. Bochkareva, “High-molecular Weight Compds.” [in Russian]3, 1321 (1961).
R. O. Sauer, J. Amer. Chem. Soc.,68, 138 (1946).
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Andrianov, K.A., Pichkhadze, S.V. & Komarova, V.V. Reactions of dimethylcyclosiloxanes with butylorthotitanate. Russ Chem Bull 11, 672–673 (1962). https://doi.org/10.1007/BF00904775
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DOI: https://doi.org/10.1007/BF00904775