Conclusions
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1.
The applicability of the NMR pulse technique (spin echo) and infrared spectroscopy for characterizing sorbents of various resolving powers in the chromatography of methylated methylglycosides is investigated.
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2.
The “spin echo” technique can be used for selecting sorbents of high resolving power for the chromatography of hydrocarbon methyl derivatives.
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3.
No definite relation could be established between the infrared spectra and the chromatographic properties of the sorbents.
Literature cited
V. T. Bykov and A. V. Vas'kovskaya, Natural Sorbents [in Russian], Nauka,1967, p. 214.
V. T. Bykov, A. A. Vaskovskaya, and V. E. Vaskovsky, J. Chromatog.,30, 643 (1967).
E. L. Hahn, Phys. Rev.,80, 580 (1950).
V. D. Korepanov and A. I. Chernitsyn, Symposium on Paramagnetic Resonance [in Russian], Izd-vo Kazanskogo gos. un-ta, 1964, p. 134.
J. R. Zimmerman and W. E. Brittin, J. Phys. Chem.,61, 1328 (1957).
J. R. Zimmerman and J. A. Lasater, J. Phys. Chem.,62, 1157 (1958).
D. E. Woessner, J. Chem. Phys.,39, (11), 2783 (1963).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 11, pp. 2636–2639, November, 1968.
The infrared spectra were obtained by V. E. Odinokov whom the authors would like to thank.
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Bykov, V.T., Vas'kovskaya, A.A. & Chernitsyn, A.I. Resolving power of natural adsorbents in the chromatogeaphy of methylated methylglycosides. Russ Chem Bull 17, 2501–2503 (1968). https://doi.org/10.1007/BF00903417
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DOI: https://doi.org/10.1007/BF00903417