Synthesis of thiophosphoryl-substituted derivatives of cycloalkanecarboxylic acids

  • P. V. Kazakov
  • I. L. Odinets
  • P. V. Petrovskii
  • L. V. Kovalenko
  • T. A. Mastryukova
Organic Chemistry Methods Of Synthesis

Abstract

The 1-thiophosphorylated esters and nitriles of cycloalkanecarboxylic acids were obtained both by the direct reaction of derivatives of thiophosphorylacetic acids with α,ω-dihalogenoalkanes in the K2CO3/DMSO heterophasic system, and as a result of the reaction of the corresponding oxygen compounds with the Louson reagent.

Keywords

cycloalkylthiophosphonates cycloalkylthiophosphinates cycloalkylphosphine sulfides thiophosphorylacetic acids cycloalkylation Louson reagent 

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Copyright information

© Plenum Publishing Corporation 1992

Authors and Affiliations

  • P. V. Kazakov
  • I. L. Odinets
  • P. V. Petrovskii
  • L. V. Kovalenko
  • T. A. Mastryukova

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