Summary
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1.
Derivatives of N-diethylphosphoryliminothiocarbamic acid have been obtained by the action of ammonia and methylamine, ethylamine, and diethylamine on the monochlorides of N-diethylphosphorylimino-S-alkylcarbonic acids (alkyl groups: C2H5, i-C3H7, C3H7, C4H9) and have been characterized.
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2.
The reaction of triethyl and tripropyl phosphites with the dichloride of N-diethylphosphoryliminocarbonic acid has given the corresponding bis-C-[O,O-dialkylphosphoryl]-methyleneamides of diethylphosphoric acid.
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3.
The reaction of dimethylamine and diethylamine with the dichloride of N-[N′,N′,N″,N″-tetramethyldiamidophosphoryl]-iminocarbonic acid forms the corresponding N-phosphorylimidotetraalkylureas.
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Literature cited
P. I. Alimov and L. N. Levkova, Izv. AN SSSR, Ser. khim., 187, 932, 1189 (1964).
P. I. Alimov and L. N. Levkova, Izv. AN SSSR, Ser. khim., 1298 (1965).
J. Michalski, H. Strzelecka, and J. Wieczorkowski, Roczniki Chem.31, 879 (1957); Chem. Abstrs.,52, 8037i (1958).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2218–2220, December, 1966.
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Levkova, L.N., Alimov, P.I. Synthesis of derivatives of N-phosphoryliminothiocareamic acid and N-phosphorylimidourea. Russ Chem Bull 15, 2149–2151 (1966). https://doi.org/10.1007/BF00867722
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DOI: https://doi.org/10.1007/BF00867722