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Coulometric method for the microdetermination of active hydrogen in organic compounds

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

An automatic, simple, and rapid coulometric method is proposed for the microdetermination of active hydrogen in organic compounds. The method is based on the reaction of active hydrogen with LiAlH4, combustion of the hydrogen formed to water, and measurement of the amount of electricity expended in its electrolysis.

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Literature cited

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, USSR

    G. F. Anisimova & V. A. Klimova

Authors
  1. G. F. Anisimova
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  2. V. A. Klimova
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 581–583, March, 1972.

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Anisimova, G.F., Klimova, V.A. Coulometric method for the microdetermination of active hydrogen in organic compounds. Russ Chem Bull 21, 538–540 (1972). https://doi.org/10.1007/BF00863196

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  • DOI: https://doi.org/10.1007/BF00863196

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