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1,1,4,4-Tetranitrobutane-2,3-diol and its derivatives. 4. Study of the reaction of 1,1,4,4-tetranitrobutane-2,3-diol with N-(methoxymethyl)-2-fluoro-2,2-dinitroethylamine; synthesis and crystalline structure of 1,12-difluoro-1,1,3,5,5,8,8,10,12,12-decanitro-3,10-diazadodecane-6,7-diol dinitrate

  • Organic Chemistry
  • Methods Of Synthesis
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Bulletin of the Russian Academy of Sciences, Division of chemical science Aims and scope

Abstract

A two-step synthesis has been proposed to obtain 1,12-difluoro-1,1,3,5,5,8,8,10,12,12-decanitro-3,10-diazadodecane-6,7-diol dinitrate, starting from 1,1,4,4-tetranitrobutane-2,3-diol and N-(methoxymethyl)-2-fluoro-2,2-dinitroethyl-amine, followed by nitration of the Mannich base formed. An x-ray-diffraction investigation of the dinitrate obtained was carried out.

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Literature cited

  1. B. S. Fedorov, V. V. Arakcheeva, and L. T. Eremenko,Izv. Akad. Nauk SSR, Ser. Khim., No. 3, 721 (1989).

  2. B. S. Fedorov, N. I. Golovina, L. S. Barinova, V. V. Arakcheeva, R. F. Trofimova, and L. O. Atovmyan,Izv. Akad. Nauk SSSR, Ser. Khim., No. 3, 664 (1992).

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Authors
  1. B. S. Fedorov
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  2. N. I. Golovina
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  3. V. V. Arakcheeva
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  4. G. V. Shilov
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  5. L. O. Atovmyan
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Additional information

Insitute of Chemical Physics, Russian Academy of Sciences, 142432 Chernogolovka. Translated from Izvestiya Akademii Nauk, Seriya Khimicheskaya, No. 3, pp. 671–675, March, 1992.

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Fedorov, B.S., Golovina, N.I., Arakcheeva, V.V. et al. 1,1,4,4-Tetranitrobutane-2,3-diol and its derivatives. 4. Study of the reaction of 1,1,4,4-tetranitrobutane-2,3-diol with N-(methoxymethyl)-2-fluoro-2,2-dinitroethylamine; synthesis and crystalline structure of 1,12-difluoro-1,1,3,5,5,8,8,10,12,12-decanitro-3,10-diazadodecane-6,7-diol dinitrate. Russ Chem Bull 41, 528–530 (1992). https://doi.org/10.1007/BF00863077

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  • DOI: https://doi.org/10.1007/BF00863077

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