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First step of reaction for formation of oxaphospholanols

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

The reaction ofβ-acetoethyl alcohol with alkyl dichlorophosphites in the presence of triethylamine gave alkyl di-(γ-ketobutyl)-phosphites, which confirms the first step of the previously proposed scheme for the reaction of diacetone alcohol with the dichlorides of trivalent phosphorus acids.

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Literature cited

  1. N. I. Rizpolozhenskii, F. S. Mukhametov, and R. R. Shagidullin, Izv. Akad. Nauk SSSR, Ser. Khim., 1121 (1969).

  2. L. J. Bellamy, The Infrared Spectra of Complex Molecules [Russian translation], IL (1963).

  3. V. Mark, C. H. Dungan, M. M. Crutchfield, and J. R. Van Wazer, Top. Phosphorus Chem.,5, 227 (1967); C. A.,68, 91269c (1968).

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Authors and Affiliations

  1. A. E. Arbuzov Institute of Organic and Physical Chemistry, Academy of Sciences of the USSR, USSR

    N. I. Rizpolozhenskii & F. S. Mukhametov

Authors
  1. N. I. Rizpolozhenskii
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  2. F. S. Mukhametov
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 1, pp. 175–176, January, 1972.

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Rizpolozhenskii, N.I., Mukhametov, F.S. First step of reaction for formation of oxaphospholanols. Russ Chem Bull 21, 163–164 (1972). https://doi.org/10.1007/BF00855681

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  • DOI: https://doi.org/10.1007/BF00855681

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