Conclusions
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1.
The crystals of rubidium ozonide belong to the monoclinic system. The cell parameters were determined.
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2.
Based on the x-ray phase analysis data, ozonized RbO2 is a mixture of the ordinary modifications of RbO2 and RbO3, and they fail to exhibit mutual solubility. It is postulated that amorphous RbO2 is formed during the decomposition of RbO3.
Literature cited
M. S. Dobrolyubova, Dissertation [in Russian], Moscow (1970).
A. B. Tsentsiper and M. S. Dobrolyubova, Izv. Akad. Nauk SSSR, Ser. Khim., 1471 (1972).
M. S. Dobrolyubova, T. I. Rogozhnikova, and A. B. Tsentsiper, Zh. Analit. Khim.,26, 2257 (1971).
A. Helms and W. Klemm, Z. Anorg. Allgem. Chem.,241, 97 (1939).
S. S. Gorelik, L. N. Rastorguev, and Yu. A. Skakov, X-Ray and Electron-Optical Analysis [in Russian], Metallurgiya (1970), p. 111.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 1, pp. 146–148, January, 1973.
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Dobrolyubova, M.S., Dudarev, V.Y., Sarin, V.A. et al. Thermal decomposition of ozonized rubidium hyperoxide. Russ Chem Bull 22, 145–146 (1973). https://doi.org/10.1007/BF00854143
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DOI: https://doi.org/10.1007/BF00854143