Conclusions
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1.
Ethyl fluoronitroacetate was synthesized by the direct fluorination of ethyl nitroacetate and its principal physicochemical characteristics were described.
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2.
The ethyl ester ofα-fluoro-α-nitro-β-hydroxypropionic acid and its acetate were synthesized.
Literature cited
H. Shechter and E. B. Roberson, J. Org. Chem.,25, 175 (1960).
V. Grakauskas and K. Baum, J. Org. Chem.,33, 3080 (1968).
H. G. Adolph, R. E. Oesterling, and M. E. Sitzmann, J. Org. Chem.,33, 4296 (1968).
L. T. Eremenko and G. V. Oreshko, Izv. Akad. Nauk SSSR, Ser. Khim. 380 (1969).
Organic Syntheses, Collective [Russian translation], Vol. 1, Izd. AN SSSR, Moscow-Leningrad (1950).
E. R. Bissell, J. Org. Chem.,26, 5100 (1961).
A. V. Fokin, V. S. Galakhov, and V. P. Radchenko, Zh. Obshch. Khim.,39, 1345 (1969).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2791–2793, December, 1971.
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Oreshko, G.V., Eremenko, L.T. Direct fluorination of ethyl nitroacetate. Russ Chem Bull 20, 2646–2648 (1971). https://doi.org/10.1007/BF00853642
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DOI: https://doi.org/10.1007/BF00853642