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Synthesis and properties of pyrimidinylalkylphosphonic acids

Communication 5. Synthesis ofβ-(oxopyrimidinyl-n)-ethylphosphonic acids

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    A study was made of the reaction of 3-(β-chloroethyl)-6-methyluracil and 1,3-bis-(β-chloroethyl)-6-methyluracil with triethyl phosphite.

  2. 2.

    A study was made of the reaction of 3-(β-hydroxyethyl)-6-methyluracil, 1,3-bis-(β-hydroxyethyl)-6-methyluracil and 2-amino-4-oxo-3-(β-hydroxyethyl)-6-methyl-3,4-dihydropyrimidine with triphenyl phosphite.

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Literature cited

  1. V. S. Reznik and Yu. S. Shvetsov, Izv. Akad. Nauk SSSR, Ser. Khim., 2231 (1971).

  2. V. S. Reznik, N. G. Pashkurov, O. A. Raevskii, and Yu. S. Shvetsov, Izv. Akad. Nauk SSSR, Ser. Khim., 919 (1969).

  3. A. F. Grapov, Reactions and Methods of Study of Organic Compounds [in Russian], Vol.15, Khimiya (1966), p. 67.

  4. J. R. Ferraro, D. F. Peppard, and G. W. Mason, J. Inorg. Nucl. Chem.,27, 2055 (1965).

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  5. V. S. Reznik and Yu. S. Shvetsov, Izv. Akad. Nauk SSSR, Ser. Khim., 2254 (1970).

  6. B. A. Khaskin, Reactions and Methods of Study of Organic Compounds [in Russian], Vol.20, Khimiya (1969), p. 141.

  7. L. J. Bellamy, Infared Spectra of Complex Molecules [Russian translation], IL (1957).

  8. G. M. Kosolapoff, Organophosphorus Compounds, New York-London (1950), p.202.

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Authors and Affiliations

  1. A. E. Arbuzov Institute of Organic and Physical Chemistry, Academy of Sciences of the USSR, USSR

    V. S. Raznik, Yu. S. Shvetsov & N. G. Pashkurov

Authors
  1. V. S. Raznik
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  2. Yu. S. Shvetsov
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  3. N. G. Pashkurov
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 402–406, February, 1973.

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Raznik, V.S., Shvetsov, Y.S. & Pashkurov, N.G. Synthesis and properties of pyrimidinylalkylphosphonic acids. Russ Chem Bull 22, 382–385 (1973). https://doi.org/10.1007/BF00850996

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  • DOI: https://doi.org/10.1007/BF00850996

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