Skip to main content
SpringerLink
Log in

The use of gas chromatography to separate aliphatic unsaturated sulfur-containing compounds

  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The conditions of high-temperature gas chromatography of substances containing sulfur simultaneously in the form of sulfide and sulfone groups in conjunction with a double bond on filled columns with an efficiency of 4500–5000 theoretical plates were developed.

  2. 2.

    The quantitative results obtained with a flame-ionization detector in the chromatography of isomeric sulfur-containing compounds correspond to the true composition of the mixture to be analyzed.

  3. 3.

    The separation of cis- and trans-isomers of ethyl-β-bromovinyl sulfides by the method of preparative gas chromatography was accomplished for the first time.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. P. P. Alikhanov and L. Ya. Moshkova, in: Gas Chromatography [in Russian], Vol. 3, Moscow (1965), p. 156.

    Google Scholar 

  2. V. E. Gates and C. E. Melloan, J. Chromatogr.,11, 472 (1963).

    PubMed  Google Scholar 

  3. V. E. Gates and C. E. Melloan, Analyt. Chem.,35, 658 (1963).

    Google Scholar 

  4. J. Petranek, J. Chromatogr.,5, 254 (1961).

    Google Scholar 

  5. E. N. Prilezhaeva, V. I. Laba, V. I. Snegotskii, and R. I. Shekhtman, Izv. Akad. Nauk SSSR, Ser. Khim., 1602 (1970).

  6. J. F. Arens and T. Doornbos, Recueil Trav. Chim.,75, 481 (1956).

    Google Scholar 

  7. B. A. Rudenko, A. A. Naravyan, and V. F. Kucherov, Zh. Analit. Khimii,23, 114 (1968).

    Google Scholar 

  8. E. C. Horning, E. A. Moscatelly, and C. C. Swelly, Chem. Industr.,25, 751 (1959).

    Google Scholar 

  9. R. K. Beerthuis and J. H. Recourt, Nature,186, 372 (1960).

    PubMed  Google Scholar 

  10. J. Bohemen, S. H. Longer, R. H. Perrett, and J. H. Purnell, J. Chem. Soc., 2444 (1960).

  11. D. M. Ottenstein, J. Gas Chromatogr.,6, 129 (1968).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, USSR

    E. N. Prilezhaeva, R. I. Shekhtman, B. A. Rudenko, V. I. Snegotskii & V. I. Laba

Authors
  1. E. N. Prilezhaeva
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. R. I. Shekhtman
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. B. A. Rudenko
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. I. Snegotskii
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. V. I. Laba
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 9, pp. 1945–1949, September, 1970.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Prilezhaeva, E.N., Shekhtman, R.I., Rudenko, B.A. et al. The use of gas chromatography to separate aliphatic unsaturated sulfur-containing compounds. Russ Chem Bull 19, 1831–1834 (1970). https://doi.org/10.1007/BF00849754

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00849754

Keywords

Search

Navigation