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Determination of oxygen with a flame-ionization detector

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    A gas-chromatographic method was proposed for determining oxygen using a flame-ionization detector, after quantitative conversion of the oxygen to carbon monoxide on charcoal and reduction of the carbon monoxide to methane in a stream of hydrogen on a nickel catalyst. The resolution of the method comprises 2.10−9 M oxygen; reproducibility of the results of the analysis ± 5% rel.

  2. 2.

    An example of the analysis of a mixture of oxygen and hydrocarbons on a chromatographic setup with a flame-ionization detector is cited.

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Authors and Affiliations

  1. Institute of Petrochemical Synthesis, Academy of Sciences, USSR

    V. G. Berezkin, A. E. Mysak & L. S. Polak

Authors
  1. V. G. Berezkin
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  2. A. E. Mysak
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  3. L. S. Polak
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seria Khimicheskaya, No. 10, pp. 1871–1873, October, 1964

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Berezkin, V.G., Mysak, A.E. & Polak, L.S. Determination of oxygen with a flame-ionization detector. Russ Chem Bull 13, 1769–1771 (1964). https://doi.org/10.1007/BF00849446

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  • DOI: https://doi.org/10.1007/BF00849446

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