Synthesis of esters of n-phosphorylated imidothiocarbonic and imidocarbonic acids
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The reaction of diethylphosphoric acid dichloromethyleneamide with the ethyl, propyl, isopropyl, butyl and benzyl mercaptides of sodium gave the corresponding dithioalkyl derivatives of the methyleneamidophosphate.
The reaction of diethylphosphoric acid dichloromethyleneamide with sodium glycolate gave the cyclic ethylene glycol methyleneamide of the same acid.
When diethylphosphoric acid in thiopropylmonochloromethyleneamide was reacted with propylmagnesium bromide or with ethylenimine we isolated and characterized the corresponding mixed methyleneamidophosphate derivatives.
KeywordsSodium Ethylene Ester Ethyl Bromide
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- 1.P. I. Alimov and L. N. Levkova, Izv. AN SSSR, Ser. Khim.,1964, 1889.Google Scholar