Summary
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1.
Perfluoro-tert-butylhydroxylamine was obtained by the hydrogenation of perfluoro-tert-nitrosobutane over Pd-black.
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2.
Perfluoro-tert-butylamine was obtained by the reduction of perfluoro-tert-butylhydroxylamine with hydriodic acid.
Literature cited
B. L. Dyatkin and B. P. Mochalina, Izv. AN SSSR, Ser. Khim.,1965, 926.
I. L. Knunyants and B. L. Dyatkin, Izv. AN SSSR, Ser. Khim.,1964, 923.
I. L. Knunyants, E. G. Bykhovskaya, V. N. Frosin, and Ya. M. Kisel, Dokl. AN SSSR,132, 123 (1960).
E. G. Bykhovskaya, Dissertation [in Russian], Moscow (1963).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 6, pp. 1091–1093, June, 1965
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Knunyants, I.L., Dyatkin, B.L. & Mochalina, E.P. Perfluoro-tert-butylamine. Russ Chem Bull 14, 1056–1058 (1965). https://doi.org/10.1007/BF00845761
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DOI: https://doi.org/10.1007/BF00845761