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Synthesis of γ-diketones by the method of conjugated hydrogenolysi s

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

1-Furylbutanol-3 and 1-furylpentanol-3 undergo conversions as the result of conjugated hydrogenolysis with hydrogenation in the vapor phase on skeletal Ni-Al at 240°-the former to hexanedione-2,5, heptanedione-2,5, and octanedione-2,5 in a total yield of 30%, the latter to heptanedione-2,5, octanedione-3,6 and nonanedione-3,6, in the same total yield.

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Literature cited

  1. I. F. Bel'skii and N. I. Shuikin, Dokl. AN SSSR128, 945 (1959).

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  3. I. F. Bel'skii Izv. AN SSSR, Otd. Khim. N.1962, 142.

  4. N. I. Shuikin and I. F. Bel'skii, Dokl. AN SSSR,131, 109 (1960).

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  5. N. I. Shuikin and I. F. Bel'skii, Dokl. AN SSSR115, 330 (1957).

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences, USSR

    N. I. Shuikin, I. F. Bel'skii, R. A. Karakhanov & A. A. Nazaryan

Authors
  1. N. I. Shuikin
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  2. I. F. Bel'skii
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  3. R. A. Karakhanov
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  4. A. A. Nazaryan
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Shuikin, N.I., Bel'skii, I.F., Karakhanov, R.A. et al. Synthesis of γ-diketones by the method of conjugated hydrogenolysi s. Russ Chem Bull 13, 697–698 (1964). https://doi.org/10.1007/BF00845326

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  • DOI: https://doi.org/10.1007/BF00845326

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