Summary
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1.
The reaction of condensation of dialdehyde cellulose with nitromethane with formation of a seven membered ring occurs in aqueous alkaline medium containing NaOH in amounts of 0.5–1 equivalent for each CHO group of the dialdehyde cellulose.
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2.
Condensation of dialdehyde cellulose with nitroethane, nitroethanol, and 2-nitro-1,3-propanediol, gave new cellulose derivatives with a secondary and tertiary nitro group.
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Literature cited
Z. I. Kuznetsova, V. S. Ivanova, and N. N. Shorygina, Izv. AN SSSR, Otd. khim. n., 1962, 2087.
Advances in Carbohydrate Chem.,16, 146, 1961.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12 p. 2232–2235, December, 1964
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Kuznetsova, Z.I., Ivanova, V.S. & Shorygina, N.N. The preparation of some derivatives of cellulose which contain NO2 groups. Russ Chem Bull 13, 2135–2137 (1964). https://doi.org/10.1007/BF00844239
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DOI: https://doi.org/10.1007/BF00844239