Skip to main content
Log in

Preparative synthesis of 2,2,6,6-tetramethyl-4-oxopiperidin-1-oxyl

  • Brief Communications
  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

When triacetonamine was slowly oxidized with an aqueous solution of hydrogen peroxide in the presence of sodium tungstate at room temperature, 2,2,6,6-tetramethyl-4-oxopiperidin-1-oxyl was obtained in good yield.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Literature cited

  1. Patent FRG 951933, 1956.

  2. O. L. Lebedev, M. L. Khidekel', andG. A. Razuvaev, Dokl. AN SSSR,140, 1327 (1961).

    Google Scholar 

  3. M. B. Neiman, Yu. G. Mamedova, and é. G. Rozantsev, Azerb. khim. zh., No. 6, 37 (1962).

    Google Scholar 

  4. I. I. Levantovskaya, B. M. Neiman, é. G. Rozantsev, and M. P. Yazvikova, Plast. Massy, No. 3, 14 (1964).

    Google Scholar 

  5. M. B. Neiman, A. A. Medzhikov, é. G. Rozantsev, and L. A. Skripko, Dokl. AN SSSR,154, 387 (1964).

    Google Scholar 

  6. M. B. Neiman, é. G. Rozantsev, and Yu. G. Mamedova, Nature,200, 256 (1963).

    Google Scholar 

  7. M. B. Neiman, é. G. Rozantsev, and Yu. G. Mamedova, Nature,196, 472 (1962).

    Google Scholar 

  8. N. P. Konovalova, G. N. Bogdanov, V. B. Miller, M. B. Neiman, é. G. Rozantsev, and N. M. émanuél', Dokl. AN SSSR,157, 707 (1964).

    Google Scholar 

  9. M. B. Neiman, é. G. Rozantsev, Izv. AN SSSR Ser. khim., 1964, 1178.

  10. M. B. Neiman, S. G. Maironovskii, B. M. Kovarskaya, é. G. Rozantsev, and é. G. Grinberg, Izv. AN SSSR Ser. khim., 1964, 1518.

  11. H. K. Hall, J. Amer. Chem. Soc.,79, 5444 (1957).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12 p. 2218, December, 1964

Rights and permissions

Reprints and permissions

About this article

Cite this article

Rozantsev, é.G. Preparative synthesis of 2,2,6,6-tetramethyl-4-oxopiperidin-1-oxyl. Russ Chem Bull 13, 2117 (1964). https://doi.org/10.1007/BF00844230

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00844230

Keywords

Navigation