Monatshefte für Chemie / Chemical Monthly

, Volume 116, Issue 11, pp 1275–1289 | Cite as

Nioboxidfluoride mit Blockstrukturen — Elektronenmikroskopische Durchstrahlungsaufnahmen und ihre Simulation

29. Mitteilung über „Beiträge zur Untersuchung anorganischer nichtstöchiometrischer Verbindungen“
  • Birgit Langenbach-Kuttert
  • Ronald Roß
  • Reginald Gruehn
Anorganische Und Physikalische Chemie

Niobiumoxidefluorides with blockstructures—High resolution electron microscopical images and their simulation

Abstract

Niobiumoxidefluorides Nb59O147F, Nb31O77F, Nb65O161F3 and Nb34O84F2 were prepared by reaction of Nb2O5 and Nb3O7F at 1 270°C. These niobiumoxidefluorides have blockstructures which were examined by high resolution electron microscopy. The observed images of the crystal structures were compared with computer simulated images.

Keywords

Niobiumoxidefluoride Blockstructure High resolution electron microscopy Image simulation 

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Literatur

  1. 1.
    28. Mitt.:Reitz B., Gruehn R., Naturwissenschaften71, 474 (1984).Google Scholar
  2. 2.
    Gruehn R., NBS Spec. Publ.364, Solid State Chem., Proc. of 5th Mater. Res. Symp. July 1972.Google Scholar
  3. 3.
    Wadsley A. D.,Andersson S., in: Perspectives in Structural Chemistry, Vol. III, 1 (1970).Google Scholar
  4. 4.
    Wadsley A. D., Acta Cryst.14, 660 (1961).Google Scholar
  5. 5.
    Gatehouse B. M., Wadsley A. D., Acta Cryst.17, 1545 (1964).Google Scholar
  6. 6.
    Allpress J. G., Sanders J. V., Wadsley A. D., Phys. Stat. Sol.25, 541 (1968).Google Scholar
  7. 7.
    Mertin W., Philips Bulletin Electron Optics EM112, 1979/1.Google Scholar
  8. 8.
    Gruehn R., Mertin W., Angew. Chem.92, 531 (1980).Google Scholar
  9. 9.
    Gruehn R., Mertin W., Naturwissenschaften69, 53 (1982).Google Scholar
  10. 10.
    Heurung G., Gruehn R., Z. anorg. allg. Chem.491, 101 (1982).Google Scholar
  11. 11.
    Allpress J. G., J. Solid State Chem.1, 66 (1969).Google Scholar
  12. 12.
    Norin R., Acta Chem. Scand.25, 347 (1971).Google Scholar
  13. 13.
    Åstroem A., Acta Chem. Scand.20, 969 (1966).Google Scholar
  14. 14.
    Wadsley A. D., Rev. Pure Appl. Chem. (Australien)5, 165 (1965).Google Scholar
  15. 15.
    Hibst H., Gruehn R., Z. Naturforsch.33 b, 884 (1978).Google Scholar
  16. 16.
    Roth R. S., Wadsley A. D., Acta Cryst.18, 724 (1965).Google Scholar
  17. 17.
    Gruehn R., Z. anorg. allg. Chem.395, 181 (1973).Google Scholar
  18. 18.
    Roß R., Gruehn R., Z. Naturforsch.39 b, 19 (1984).Google Scholar
  19. 19.
    Krämer E., Dissertation, Gießen 1976.Google Scholar
  20. 20.
    Andersson S., Acta Chem. Scand.19, 1401 (1965).Google Scholar
  21. 21.
    Skarnulis A. J., Dissertation, Arizona State University 1976.Google Scholar
  22. 22.
    Heidenreich R. D., Fundamentals of Transmission Electron Microscopy. New York: Interscience—Wiley. 1964.Google Scholar
  23. 23.
    Cowley J. M., Diffraction Physics. Amsterdam: North-Holland. 1975.Google Scholar
  24. 24.
    Goodman P., Moodie A. F., Acta Cryst.A 30, 280 (1974).Google Scholar
  25. 25.
    Langenbach-Kuttert B., Mertin W., Z. Krist.170, 115 (1985).Google Scholar
  26. 26.
    Langenbach-Kuttert B.,Mertin W.,Gruehn R., in Vorbereitung.Google Scholar

Copyright information

© Springer-Verlag 1985

Authors and Affiliations

  • Birgit Langenbach-Kuttert
    • 1
  • Ronald Roß
    • 1
  • Reginald Gruehn
    • 1
  1. 1.Institut für Anorganische und Analytische ChemieJustus-Liebig-Universität GießenGießenBundesrepublik Deutschland

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