Abstract
The dislocation structure of NiO single crystals used in diffusion studies has been examined by transmission electron microscopy. The crystals contain dislocations (the dislocation density being 4 × 1012 m−2) that are probably a result of the growth process. The dislocations have a Burgers vector ofa/2 〈110〉. On annealing at temperatures above 1400° C the density is reduced to ∼ 7 × 1011 m−2, most of the dislocations forming low angle boundary arrays. The dislocation density was found to be much greater in the vicinity (within 1μm) of a mechanically polished surface.
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References
A. Atkinson andR. I. Taylor, (to be published).
G. W. Fynn, W. J. A. Powell, M. Blackman andD. Jenner,J. Phys. E. Sci. Instrum. 4 (1971) 391.
P. Delavignette andS. Amelinckx,Appl. Phys. Lett. 2 (1963) 236.
J. W. Edington, “Interpretation of Transmission Electron Micrographs” (Macmillan, London, 1975).
R. Hales,Corrosion Sci. 12 (1972) 555.
P. R. Swann, “Electron Microscopy and Strength of Materials” (Interscience New York, 1963) p. 131.
F. C. Frank, “Defects in Crystalline Solids” (Phys. Soc., London, 1955) p. 159.
B. J. Hockey,Proc. Brit. Ceram. Soc. 20 (1972) 91.
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Sears, J.S. Transmission electron microscopy of dislocations in nickel oxide single crystals. J Mater Sci 13, 2455–2461 (1978). https://doi.org/10.1007/BF00808061
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DOI: https://doi.org/10.1007/BF00808061