Abstract
A synthesis of enantiomeric pure (2R)-1-oxo-2-methyl-oxazine (3), starting fromL-2-Chloropropionic isobutylester and ethanolamine is reported.
Literatur
Lehr M., Karlan S., Goldberg M. W., J. Med. Chem.6, 136 (1963).
Surrey A. R., Winthrop S. O., Rukwid M. K., Tullar B. J., J. Amer. Chem. Soc.77, 633 (1955).
Maillard J.,Vincent M.,Delaunay P.,Ropin M.,Van-Tri V.,Remond G., Chim. Ther.1969, 80.
Albert R.,Csuk R.,Leitner E.,Weidmann H., XIIth Intern. Carbohydr. Symp., Utrecht 1984; A. 1.30.
A. P. 3092630 (1958); C.A.59, 11511 (1963).
DBP 956683; C.A.51, 9516 (1957).
Jacobs W. A., J. Amer. Chem. Soc.39, 2188 (1917).
E. P. 729441; C.A.50, 8730 (1956).
A.P. 2432393 (1945); C.A.42, 2441f (1948).
Stachel H. D., Ger. off. 2.431.734; C.A.84, 813562 (1976).
A.P. 2442345 (1945); C.A.42, 9186d (1967).
Pfeil E., Harder U., Angew. Chem.79, 188 (1967).
Vieles P.,Seguin J., Comp. rend.1952, 1980.
Testa E., Nikolaus B. J. R., Mariani L., Helv. Chim. Acta46, 766 (1963).
Freudenberg K., Markert L., Ber. Dt. Chem. Ges.60, 2447 (1927).
Fu S. C., Birnbaum S. M., Greenstein J. P., J. Amer. Chem. Soc.76, 6054 (1954).
Honkanen E., Acta Chem. Scand.14, 1214 (1960).
El-Abadelah M. M., Tetrahedron29, 589 (1973).
Imfeld M., Suchy M., Vogt P., Lukac T., Schlageter M., Widmer E., Helv. Chim. Acta65, 1233 (1982).
Bestian H., Liebigs Ann. Chem.566, 210 (1950).
Vieles M.,Seguin J., Bull. Soc. Chim. Fr.1953, 287.
Spassov S. L., Stefanovsky J. N., Kuretv B. J., Fodor G., Chem. Ber.105, 2467 (1972).
Fodor G., Stefanovsky J., Kurtev B. J., Monatsh. Chem.98, 1027 (1967).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Csuk, R. Synthese von enantiomerenreinem (2R)-1-Oxo-2-methyl-oxazin. Monatsh Chem 116, 677–680 (1985). https://doi.org/10.1007/BF00798793
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF00798793