Conclusions
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1.
A study was made of the single-stage reduction of WO3 to W in an industrial GSPI muffle furnace with a direct-flow feed of hydrogen into the furnace muffle.
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2.
It is shown that, with hydrogen supplied by the direct-flow technique, it is possible to produce in a single stage, at unchanged furnace output, a homogeneous, fine-grained tungsten powder with an adsorption of more than 0.2 mg/g and a mean particle size of < 1μ.
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3.
An investigation was carried out of the effect of sintering temperature on the properties of T15K6 alloy produced from tungsten powder prepared by the direct hydrogen flow technique.
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4.
It is shown that, compared with a standard T15K6 alloy, an alloy of the same composition produced from tungsten powder prepared in a muffle furnace with a direct-flow hydrogen supply possesses a finer-grained WC phase structure and superior physicomechanical and cutting properties.
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Literature cited
V. I. Tret'yakov, Sintered Hard Alloys [in Russian], Metallurgizdat (1962).
G. S. Kreimer, Strength of Hard Alloys, Consultants Bureau, New York (1968).
R. Kieffer and P. Schwarzkopf, Hard Alloys [Russian translation], Metallurgizdat (1957).
G. A. Meerson and A. N. Zelikman, Metallurgy of Rare Metals [in Russian], Metallurgizdat (1955).
G. A. Meerson and V. S. Panov, Izv. Akad. Nauk SSSR, Metally, No. 3, 213 (1970).
C. J. Smithells, Tungsten, Chapman & Hall, London.
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Translated from Poroshkovaya Metallurgiya, No. 6 (114), pp. 31–35, June, 1972.
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Meerson, G.A., Kreimer, G.S., Glushkov, V.N. et al. Effect of conditions of preparation of metallic tungsten on the properties of T15K6 alloy. Powder Metall Met Ceram 11, 452–455 (1972). https://doi.org/10.1007/BF00797919
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DOI: https://doi.org/10.1007/BF00797919