Skip to main content
SpringerLink
Log in

High-temperature x-ray equipment for the study of powder and dense objects

A survey

  • Published:
Soviet Powder Metallurgy and Metal Ceramics Aims and scope

Conclusions

The existing experimental models of both Debye cameras and camera attachments for x-ray diffraction apparatus enable the atomic and crystal structure of metals and alloys to be studied on heating to very high temperatures (occasionally of the order of 3000°C) in a vacuum of 10−6 torr. The camera attachments currently produced by Soviet industry are suitable for operation at temperatures up to1500°C in a vacuum of about 10−4 torr.

It is now necessary to organize production in the Soviet Union of attachments with a temperature limit of 2000°C in a vacuum of 10−6 to 10−7 torr and high-temperature vacuum Debye cameras designed for temperatures up to 1700°C and a vacuum of 10−5 to 10−5 torr.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. D. S. Bloom and N. G. Grant, J. Metals,3, 109 (1951).

    Google Scholar 

  2. V. N. Svechnikov, Yu. A. Kocherzhinskii, and G. F. Kobzenko, Problems in Metal Physics and Metallography [in Russian], No. 11 (1960), p. 28.

    Google Scholar 

  3. R. J. Ross and W. Hume-Rothery, J. Less-Common Metals,5, 258 (1963).

    Google Scholar 

  4. B. M. Vasyutinskii et al., Fiz. Metal. i Metalloved.,12, No. 5, 771 (1961).

    Google Scholar 

  5. P. Hidnert, J. Res. Natl. Std.,27, 113 (1941).

    Google Scholar 

  6. A. K. Butylenko, V. N. Gridnev, and V. N. Minakov, in: Structure and Properties of Heat-Resisting Materials [in Russian], Izd-vo Nauka (1967), p. 32.

  7. H. J. Goldschmidt, High-Temperature X-Ray Diffraction Techniques, Oosthock's Uitgevers Mij for International Union of Crystallographers, Utrecht (1964).

  8. V. A. Finkel', High-Temperature X-Ray Diffraction Studies of Metals [in Russian], Izd-vo Metallurgiya (1968).

  9. U. Strossberger, in: Handbook of X-Rays for Diffraction, Emission, Absorption, and Microscopy, New York (1967).

  10. M. M. Umanskii, Equipment for X-Ray Structural Investigations [in Russian], Fizmatgiz (1960).

  11. A.Guinier, X-Ray Diffraction of Crystals [Russian translation], Fizmatgiz (1961).

  12. D. M. Kheiker and L. S. Zevin, X-Ray Diffractometry [in Russian], Fizmatgiz (1963).

  13. P. F. Rumyantsev, I. I. Smil'gevich, and A. S. Shaposhnikov, in: Chemistry of High-Temperature Materials [in Russian], Izd-vo Nauka (1967), p. 69.

  14. E. I. Gindin and V. G. Prokhvotilov, Zavod. Lab.,24, No. 1, 106 (1958).

    Google Scholar 

  15. J. J. Hanak and A. H. Daane, Rev. Sci. Instr.,32, No. 6, 106 (1961).

    Google Scholar 

  16. B. A. Hatt et al., J. Sci. Instr.,37, No. 38, 273 (1960).

    Google Scholar 

  17. G. P. Perinet, Bull. Soc. Franc. Mineral. Cryst.,88, No. 4, 702 (1965).

    Google Scholar 

  18. J. W. Edwards et al., Rev. Sci. Instr.,20, No. 5, 343 (1949).

    Google Scholar 

  19. H. J. Goldschmidt and J. Cunningham, J. Sci. instr.,27, 177 (1950).

    Google Scholar 

  20. Continuous Cassette Moving Vacuum High-Temperature Camera, Rigaku Denki, Tokyo, Catalog No. 1821 (1966).

  21. RTVKM Multiframe X-Ray High-Temperature Vacuum Camera, Pribory dlya Nauchn. Issled., No. 2 (3), ONTIpribor (1966).

  22. Yu. A. Kocherzhinskii, V. V. Pet'kov, and V. M. Pan, Pribory i Tekh. Éksperim. No. 4, 219 (1969).

    Google Scholar 

  23. Yu. A. Kocherzhinskii, V. T. Cherepin, V. M. Pan, et al., in: Equipment and Techniques for X-Ray Analysis [in Russian], No. 5, Leningrad (1969), p. 88.

    Google Scholar 

  24. Yu. A. Kocherzhinskii, V. V. Pet'kov, et al., in: Phase Transformations [in Russian], No. 27, Izd-vo Naukova Dumka, Kiev (1970), p. 225.

    Google Scholar 

  25. Yu. A. Kocherzhinskii, V. M. Pan, G. F. Kobzenko, et al., Problems in Metal Physics and Metallography [in Russian], No. 17, 209 (1963).

    Google Scholar 

  26. A. G. Kostornov and A. I. Raichenko, Poroshkovaya Met., No. 12, 37 (1966).

    Google Scholar 

  27. A. G. Kostornov and E. T. Denisenko, Dopovidi Akad. Nauk UkrRSR, Ser. A, No. 4, 366 (1967).

    Google Scholar 

  28. W. J. Campbell, in: Handbook of X-Rays for Diffraction, Emission, Absorption, and Microscopy (ed. F. E. Kaelble), New York (1967).

  29. V. V. Zubenko, B. G. Krants, and M. M. Umanskii, Kristallografiya,11, No. 2, 311 (1966).

    Google Scholar 

  30. KRV-1200 High-Temperature X-Ray Apparatus, Operating Instructions [in Russian], V/o Tekhsnabéksport (1968).

  31. GPVT-1500 High-Temperature X-Ray Attachment (Technical Description and Operating Instructions) [in Russian], SKB RA, Leningrad (1968).

  32. V. I. Babenko, V. V. Levitin, et al., Pribory i Tekh. Éksperim. No. 1, 189 (1969).

    Google Scholar 

  33. A. G. Boganov, L. P. Makarov, and V. S. Rudenko, Advanced Scientific-Technical and Production Experience [in Russian], No. 18-65-1091/67, GOSINTI (1965).

  34. A. G. Boganov et al., Dokl. Akad. Nauk SSSR,161, No. 2, 332 (1965).

    Google Scholar 

  35. A. S. Bystrikov, Zavod. Lab.,31, No. 9, 1151 (1965).

    Google Scholar 

  36. V. A. Landa and E. M. Stepanov, Zavod. Lab.,33, No. 4, 508 (1967).

    Google Scholar 

  37. T. W. Baker, F. J. Baldock, and W. E. Spindler, J. Sci. Instr.,43, 803 (1966).

    Google Scholar 

  38. Yu. A. Kocherzhinskii, E. I. Shishkin, and L. M. Yupko, Ogneupory, No. 5, 50 (1969).

    Google Scholar 

  39. High-Temperature X-Ray Diffractometer Attachments, Rigaku Denki, Tokyo, Catalogs Nos. 2381, 2311, and 2382 (1966).

  40. I. Simura and H. Utida, Japanese Patent Cl. III, 3, No. 8999, March 4, 1961 (appl.), May 11, 1965 (publ.).

  41. W. Ostertag and G. R. Fischer, Rev. Sci. Instr.,39, No. 6, 888 (1968).

    Google Scholar 

  42. S. Stecura, Rev. Sci. Instr.,39, No. 5, 760 (1968).

    Google Scholar 

  43. H. Ebel and W. Novak, Acta Phys. Austriaca,24, No. 2, 161 (1966).

    Google Scholar 

  44. J. P. Holden, J. Sci. Instr.,41, 706 (1964).

    Google Scholar 

  45. E. A. Kellet and E. G. Steward, J. Sci. Instr.,39, 306 (1962).

    Google Scholar 

  46. R. A. Clark and T. S. M. Maclean, Electron. Eng.,36, 83 (1964).

    Google Scholar 

  47. A. Pianelli, Mem. Sci. Rev. Met.,64, No. 3, 267 (1967).

    Google Scholar 

  48. E. M. Levin and F. A. Mauer, J. Am. Ceram. Soc.,46, No. 1, 59 (1963).

    Google Scholar 

  49. T. P. Seward et al., Rev. Sci. Instr.,36, No. 12, 1851 (1965).

    Google Scholar 

  50. M. Semlitsch, Prakt. Metallog.,4, No. 10, 503 (1967).

    Google Scholar 

  51. E. A. Harper, J. Sci. Instr., E2, No. 9, 807 (1969).

    Google Scholar 

  52. L. Guichet, Compt. Rend. Acad. Sci., AB262, No. 14, 968 (1966).

    Google Scholar 

  53. A. F. Bessonov and V. M. Ust'yantsev, Zavod. Lab.,32, No. 9, 1158 (1966).

    Google Scholar 

  54. A. F. Bessonov et al., Poroshkovaya Met., No. 3, 92 (1967).

    Google Scholar 

  55. High-Temperature Attachment for X-Ray Diffractometry-Differential Thermal Analysis, Rigaku Denki, Tokyo, Catalog No. 2971 (1966).

  56. O. Hidso, U. Hirosi, Yu. Tosikatsu, and M. Gotiro, J. Chem. Soc. Japan Ind. Chenu Soc., 69, No. 9, 1646 (1966).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Metal Physics, Academy of Sciences of the Ukrainian SSR, USSR

    Yu. A. Kocherzhinskii & V. V. Pet'kov

Authors
  1. Yu. A. Kocherzhinskii
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. V. V. Pet'kov
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Poroshkovaya Metallurgiya, No. 5(89), pp. 88–102, May, 1970.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kocherzhinskii, Y.A., Pet'kov, V.V. High-temperature x-ray equipment for the study of powder and dense objects. Powder Metall Met Ceram 9, 422–432 (1970). https://doi.org/10.1007/BF00796514

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00796514

Keywords

Search

Navigation