An X-ray diffraction investigation of the reaction between molybdenum powder and manganese additions during sintering
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Diffractograms characterizing the low-temperature sintering stage exhibit a marked distortion of the Kα doublet of molybdenum, which is indicative of appreciable reaction between the manganese and the molybdenum.
After solid-phase sintering the Mo-Mn system is characterized by marked concentration heterogeneities. Increasing the duration of the sintering does not lead to full homogeneity in the system.
The Mo-Mn system is more homogeneous after liquid-phase (1300°C) than after solidphase (1200°C) sintering.
KeywordsManganese Molybdenum Marked Concentration Sinter Stage Molybdenum Powder
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