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Dependence of the degree of completeness and duration of the borothermic reduction reaction on compact density in the preparation of metallic dodecaborides

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Soviet Powder Metallurgy and Metal Ceramics Aims and scope

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Literature cited

  1. Yu. B. Paderno and V. V. Odintsov, “Preparation of metallic dodecarborides by borothermic reduction of metallic oxides,” in: Metallothermic Processes in Chemistry and Metallurgy [in Russian], Nauka, Novosibirsk (1971), pp. 39–43.

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  1. N. K. Krupskaya Kherson Pedagogic Institute, USSR

    V. V. Odintsov & L. L. Moiseenko

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  1. V. V. Odintsov
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  2. L. L. Moiseenko
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Translated from Poroshkovaya Metallurgiya, No. 10(178), pp. 33–34, October, 1977.

Thus, in reduction reactions performed in a vacuum use should be made of blanks pressed under a certain optimum pressure, which for metallic dodecaborides is 90–120 kgf/cm2. This shortens synthesis time and enables single-phase materials to be obtained.

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Odintsov, V.V., Moiseenko, L.L. Dependence of the degree of completeness and duration of the borothermic reduction reaction on compact density in the preparation of metallic dodecaborides. Powder Metall Met Ceram 16, 766–767 (1977). https://doi.org/10.1007/BF00793583

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  • DOI: https://doi.org/10.1007/BF00793583

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