Summary
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1.
The optimum compacting pressures for niobium and molybdenum are 4000–6000 daN/cm2.
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2.
The maximum compact density is secured under the following sintering conditions:
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a)
for molybdenum: temperature 2173°K, isothermal holding for 4–5 h, environment-hydrogen;
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b)
for niobium: temperature 2173°K, isothermal holding for 3–4 h, vacuum of 0.133 N/m2(l ·10−3mmHg).
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3.
Molybdenum and, particularly, niobium show little tendency to strength loss in the temperature range 293-1473°K.
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Literature cited
M. Yu. Bal'shin, Collection: investigations of Heat-Resisting Alloys [in Russian] Moscow, Acad. Sci. USSR Press, (1958), p. 339.
M. Yu. Bal'shin and Tai Shou-vei, Izv. Akad. Nauk SSSR, Otdel. Tekhn. Nauk, Met. i Toplivo,3, 73 (1961).
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Alekseeva, F.N., Matyushenko, R.S., Rakovskii, V.S. et al. The effect of technological factors on the density and strength of sintered refractory metals. Powder Metall Met Ceram 3, 292–294 (1964). https://doi.org/10.1007/BF00774173
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DOI: https://doi.org/10.1007/BF00774173