Abstract
3,4-Bis(hydroxymethyl)furan was electrolytically methoxylated during intense cooling. 4,5-Bis(hydroxymethyl)pyridazine was obtained by reaction of the methoxylation product — 2,5-dimethoxy-3,4-bis (hydroxymethyl)-2,5-dihydrofuran — with hydrazine hydrate.
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K. Yu. Novitskii, N. K. Sadovaya, and A. B. Baskina, Khim. Geterotsikl. Soed., No. 2, 57 (1970).
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K. Yu. Novitskii, N. K. Sadovaya, and Yu. K. Yur'ev, Khim. Geterotsikl. Soed.,2, 826 (1966).
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 10, pp. 1306–1307, October, 1970.
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Novitskii, K.Y., Kas'yanova, E.F. Electrolytic methoxylation of 3,4-bis(hydroxymethyl) furan and synthesis of 4,5-bis-(hydroxymethyl) pyridazine. Chem Heterocycl Compd 6, 1216–1217 (1970). https://doi.org/10.1007/BF00755059
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DOI: https://doi.org/10.1007/BF00755059